Preparation of fluorochemical surfactant acrylate
Yunfang Wang · 2004
The FSO acrylate was prepared by reacting of fluorocarbon surfactant FSO with acryloyl chloride. The purity of FSO acrylate was analyzed by gas chromatography, and the superficial characteristics of the structure were researched by infrared spectrum (IR). The effects of reactant proportion and reaction time on the yield and purity of FSO acrylate were investigated. The results show that the yield and purity of FSO acrylate is the highest when acryloyl chloride excess ratio is 105 and reaction time is 8～10 h.